Results 1 to 2 of 2

Thread: Problem with Cell Volume AccuPyc 1330

  1. #1
    Join Date
    Jan 03

    Question Problem with Cell Volume AccuPyc 1330


    I've got a Problem with the AccuPyc 1330. The volume of chamber inserted differs to the cell volume e.g. Chamber inserted 1.0 cm3 , Cell volume 3.78 cm3.

    Has anyone got the same problem or a hint for me?

    Thank you very much


  2. #2
    Paul A. Webb - Micromeritics, USA Guest

    Source of additional volume in sample chamber

    If the your AccuPyc 1330 has a 10cc standard sample chamber and you are using an insert to reduce the sample chamber volume to 1 cc, then there will be about 3 cc of dead space around the insert and pressure transducer. This space is necessary to allow free flow of gas around the insert and necessary clearance to allow the insert to be inserted and removed. Although the sample chamber cup size has been reduced to 1 cc by the insert, the total void volume remaining in the 10 cc sample chamber is larger and equals the 1 cc cup size plus the dead space. Your unit is responding normally.

    Dead space offset always is associated with use of an insert, regardless of the size of the standard cell that came with the pycnometer. If you measure your chamber without an insert, then the result should be the size of the standard chamber. Only a 1 cc standard chamber is expected to measure 1 cc.

Similar Threads

  1. Historical Overview of the Indicizers and Jenike Shear Cell
    By Jerry R. Johanson, Ph.D. in forum Measurement and Control
    Replies: 5
    Last Post: 24th April 2015, 14:00
  2. Bark Screw Trough Wear Problem
    By Wayne W in forum Wear & Abrasion Problems
    Replies: 4
    Last Post: 22nd November 2006, 20:06
  3. Bark Screw Trough Wear Problem
    By Wayne W in forum Mechanical Conveying
    Replies: 15
    Last Post: 9th February 2005, 8:20
  4. Problem of Mixing in Powder Coatings
    By andrea in forum Flow Properties
    Replies: 2
    Last Post: 24th June 2003, 8:55
  5. Density (volume) determinations
    By Paul A. Webb - Micromeritics, USA in forum Particle Characterization & Analysis
    Replies: 0
    Last Post: 10th December 2001, 17:01

Tags for this Thread

Posting Permissions

  • You may not post new threads
  • You may not post replies
  • You may not post attachments
  • You may not edit your posts
Single Sign On provided by vBSSO